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Procedure-SolidSamplesInstrumentcalibration/driftcorrection.Placethecalibration/driftstandardina***NickelBasket,andifapplicable,placethesampleintotheappropriateautoloaderposition.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Note:samplesusingautomationshouldbeplacedintheappropriateautoloaderpositionbeforestartingtheanalysissequence.Oncethesequencehasstarted,theautomaticanalysiswillstartandendautomatically.上海禹重实业有限公司致力于提供分析仪，有需要可以联系我司哦！杭州化学分析仪咨询报价

Procedure-SolidSamplesPresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleanerAddapproximately0.05gof***GraphitePowdertoa***GraphiteCrucible.Firmlyplacethecrucibleonthelowerelectrodetiporappropriateautoloaderposition.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically六安力可LECO氧氮氢分析仪厂家报价上海禹重实业有限公司是一家专业提供分析仪的公司，有需求可以来电咨询！

Procedure-SolidSamplesPreparetheinstrumentasoutlinedintheoperatorsinstructionmanual.Determinetheinstrumentblank.Loginaminimumof3Blankreplicates.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Placea502-344NickelBasketintotheloadinghead.Note:samplesusingautomationshouldbeplacedintheappropriateautoloaderpositionbeforestartingtheanalysissequence.Oncethesequencehasstarted,theautomaticanalysiswillstartandendautomatically.

SamplePreparationSamplingandsamplepreparationofrefractorymetalssuchastitaniumandzirconiumissomewhatdifferentfromthatofsteel.Unlikesteelsamples,hydrogenisnotasmobileinthisgroupofmaterials;therefore,storageinliquidnitrogenordryiceisnotrequired.However,itisimportanttokeepthesamplecoolwhencuttingorsectioning.Samplepreparationforoxygenandnitrogendeterminationhasbeendifferentfromthatofhydrogendetermination.上海禹重实业有限公司为您提供分析仪。

SummaryThedeterminationoftheamountofoxygen,nitrogen,andhydrogeniniron,steel,nickel-,andcobalt-basealloysrepresentssomeofthemostimportantqualitymetricsforthesematerials.Oxygenisusedtocreatesteelfrompigironbyremovingexcesscarbon.Oxygencontentmustbecontrolledtolimittheamountofcarbonmonoxidethatcanbeformedduringsolidificationwhichmaycauseexcessiveporosity.Nitrogenisconsideredbothanimpurityaswellasanimportantalloyingagent.Itcanbepresentasanitrideorinterstitiallyinitsgaseousform.Increasednitrogencontentisknowntoincreaseyieldandtensilestrength,thusdecreasingductilityandformability.Excessivelevelsmayevolveduringsolidificationthusincreasingporosity.Highhydrogencontentistheprimarycauseofembrittlement,blisteringandflakingduetoitshighmobilitythroughthelatticeandprovidesnopotentialalloyingbenefits.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.上海禹重实业有限公司为您提供分析仪，有想法的可以来电咨询！力可LECO氧氮氢分析仪厂家直销

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氧氮氢分析仪的常见故障及解决方法：氧和氮空白值超过20。这是由于气流小，不能将炉子中的空气驱赶出去。可调节气体流量，调节载气压力在0.2~0.4MPa。接通仪器载气，放一个石墨坩埚在下电极上，打开主电源开关，点击软件上的关炉按钮，关闭炉子并等待10s。调节流量调节器，直到流量计a显示为30L／h，打开炉子。调节调节器直到流量计b显示为50L／h，再次关闭炉子。如果以上设置不稳定，则增加流量至100L／h，反复调节直至仪器稳定。杭州化学分析仪咨询报价

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