Procedure-SolidSamplesInstrumentcalibration/driftcorrection.Placethecalibration/driftstandardina***NickelBasket,andifapplicable,placethesampleintotheappropriateautoloaderposition.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Note:samplesusingautomationshouldbeplacedintheappropriateautoloaderpositionbeforestartingtheanalysissequence.Oncethesequencehasstarted,theautomaticanalysiswillstartandendautomatically.上海禹重实业有限公司致力于提供分析仪,有需求可以来电咨询!盐城力可分析仪
Determinetheinstrumentblank.a.Loginaminimumof3Blankreplicates.b.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.c.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.d.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.e.Firmlyplaceagraphitecrucibleonthelowerelectrodetip.f.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.g.Repeatsteps2bthrough2faminimumofthreetimes.h.Settheblankfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.淮南力可分析仪厂家直销上海禹重实业有限公司致力于提供分析仪,欢迎您的来电!
Procedure-SolidSamplesPreparetheinstrumentasoutlinedintheoperatorsinstructionmanual.Determinetheinstrumentblank.Loginaminimumof3Blankreplicates.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Placea502-344NickelBasketintotheloadinghead.Note:samplesusingautomationshouldbeplacedintheappropriateautoloaderpositionbeforestartingtheanalysissequence.Oncethesequencehasstarted,theautomaticanalysiswillstartandendautomatically.
SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.上海禹重实业有限公司致力于提供分析仪,欢迎您的来电哦!
Procedure-SolidSamples:--Instrumentcalibration/driftcorrection.Placethenickelbasketcontainingthecalibration/driftstandardintotheopenportatthetopoftheloadinghead.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.上海禹重实业有限公司是一家专业提供分析仪的公司,有需求可以来电咨询!连云港化学分析仪优惠价格
上海禹重实业有限公司是一家专业提供分析仪的公司,欢迎新老客户来电!盐城力可分析仪
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