SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.分析仪,就选上海禹重实业有限公司,用户的信赖之选,欢迎您的来电!新疆化学分析仪
Procedure-SolidSamplesInstrumentcalibration/driftcorrection.Placethecalibration/driftstandardina***NickelBasket,andifapplicable,placethesampleintotheappropriateautoloaderposition.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Note:samplesusingautomationshouldbeplacedintheappropriateautoloaderpositionbeforestartingtheanalysissequence.Oncethesequencehasstarted,theautomaticanalysiswillstartandendautomatically.山西进口力可氧氮氢分析仪采购分析仪,就选上海禹重实业有限公司,让您满意,欢迎新老客户来电!
Procedure-SolidSamplesPreparetheinstrumentasoutlinedintheoperatorsinstructionmanual.Determinetheinstrumentblank.Loginaminimumof3Blankreplicates.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Placea502-344NickelBasketintotheloadinghead.Note:samplesusingautomationshouldbeplacedintheappropriateautoloaderpositionbeforestartingtheanalysissequence.Oncethesequencehasstarted,theautomaticanalysiswillstartandendautomatically.
Instrumentcalibration/driftcorrection.a.Loginaminimumof3Standardreplicates.b.Weigha~1.000gramofacalibration/driftstandard,enterthemassandstandardidentificationintoappropriatereplicatefields.c.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.d.Placethecalibration/driftstandardintotheopenportatthetopoftheloadinghead.e.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.上海禹重实业有限公司为您提供分析仪,有需求可以来电咨询!
SummaryThedeterminationoftheamountofoxygen,nitrogen,andhydrogeniniron,steel,nickel-,andcobalt-basealloysrepresentssomeofthemostimportantqualitymetricsforthesematerials.Oxygenisusedtocreatesteelfrompigironbyremovingexcesscarbon.Oxygencontentmustbecontrolledtolimittheamountofcarbonmonoxidethatcanbeformedduringsolidificationwhichmaycauseexcessiveporosity.Nitrogenisconsideredbothanimpurityaswellasanimportantalloyingagent.Itcanbepresentasanitrideorinterstitiallyinitsgaseousform.Increasednitrogencontentisknowntoincreaseyieldandtensilestrength,thusdecreasingductilityandformability.Excessivelevelsmayevolveduringsolidificationthusincreasingporosity.Highhydrogencontentistheprimarycauseofembrittlement,blisteringandflakingduetoitshighmobilitythroughthelatticeandprovidesnopotentialalloyingbenefits.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.上海禹重实业有限公司致力于提供分析仪,有需要可以联系我司哦!江苏进口力可氧氮氢分析仪
上海禹重实业有限公司致力于提供分析仪,欢迎新老客户来电!新疆化学分析仪
ONH836系列:氧氮氢分析仪(熔融法)力可ONH836系列仪器采用惰性熔融法,提供各种无机材料、钢铁、有色金属、硬质合金、陶瓷材料中宽范围的氧氮氢同时分析。ONH836系列仪器通过采纳客户的反馈意见和创新设计,力可仪器采用触摸屏技术和在线软件平台,增强了仪器的可操作性、降低了分析成本、节省实验室桌面空间。用户友好界面的Cornerstone™软件力可的Cornerstone氧氮氧分析软件采用触摸屏界面使用户可完整的达到分析控制、方法设定、在线诊断、数据报告。Cornerstone氧氮氧分析软件允许用户在单一分析界面中完成日常的所有工作,快速而且简单易用。力可创新的批次和重复样品数据分组功能极大简化了样品结果输出和结果标准偏差的自动计算,减少了繁琐的额外数据处理。新疆化学分析仪
上海禹重实业有限公司是我国光谱仪,色谱仪,质谱仪,样品前处理专业化较早的有限责任公司(自然)之一,禹重科技是我国仪器仪表技术的研究和标准制定的重要参与者和贡献者。公司承担并建设完成仪器仪表多项重点项目,取得了明显的社会和经济效益。禹重科技将以精良的技术、优异的产品性能和完善的售后服务,满足国内外广大客户的需求。